HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formaldehyde → HCID 15701915, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | HCID 13526350 | HCID 13526350 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 15701915 | HCID 15701915 | — |
Reaction Steps
The title compound was prepared from (R)-(+)-N-1-phenylethyl-N-trimethylsilylmethylamine by reaction with n-butanol and aqueous formaldehyde following the procedure of Example 2 to give the crude acetal (85% pure) as a colourless oil (34.2 g, 84%). The nmr spectrum was identical to the above (S)-isomer.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05310911 |
| Source dataset | uspto-grants-1994_05 |
| ORD ID | ord-a3a0256718b84ea8b34df7e1b9fb8eb2 |
| Source note | uspto-grants-1994_05 |