HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1033605Erstellt: 25. Oktober 2026
2-Pentynoic acid, methyl ester → HCID 178440058, Verbindung
https://huagongshe.com/reaction/1033605
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | 2-Pentynoic acid, methyl ester | HCID 90470 | — |
| Edukt | N-Hydroxybutyramidine | HCID 2794811 | — |
| Lösungsmittel | O-Xylene | HCID 7237 | — |
| Produkt | HCID 178440058 | HCID 178440058 | 27,9% |
Reaktionsschritte
93 g of methyl pentynoate and 82 g butyramidoxime are mixed together without solvent and heated to 50° C for 24 hours. 400 mL xylene was added and water was azaeotropically removed for 6 hours. The reaction was then distilled (140° C. at 0.2 torr) to give 44 g product.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US05310929 |
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| Quelldatensatz | uspto-grants-1994_05 |
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| ORD ID | ord-9f5701372eab455db5c3bc9937b31efa |
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| Quellennotiz | uspto-grants-1994_05 |
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