1,4-Dibromobutane → HCID 19024285, compound

Participants

Reaction Steps

A solution of 84.2 mg of 2,3,4,5-tetrahydro-1,4-benzodiazepine-3,5-dione dissolved in 10 ml of dimethylformamide was ice-cooled, and then 0.0874 ml (1.5 equivalents) of 1,4-dibromobutane and 23.0 mg (1.2 equivalents) of 60% sodium hydride were added, followed reaction treatment and purification were conducted in the desired compound (yield 64%)

Provenance & Evidence