HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 6,7-Dihydro-5H-pyrrolo[3,4-b]pyridine--hydrogen chloride (1/2)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 18953638 | HCID 18953638 | — |
| Product | 6,7-Dihydro-5H-pyrrolo[3,4-b]pyridine--hydrogen chloride (1/2) | HCID 23503616 | — |
Reaction Steps
8.5 g (44 mmol) of ethyl 5,7-dihydro-1H-pyrrolo-[3,4-b]pyridine-6-carboxylate are refluxed overnight in 90 ml of concentrated hydrochloric acid. The solution is concentrated, the residue is stirred with acetone, and the salt is filtered off with suction and dried in the air.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05312823 |
| Source dataset | uspto-grants-1994_05 |
| ORD ID | ord-63017100ea8c47909c247d8996c1ec16 |
| Source note | uspto-grants-1994_05 |