HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86747869, compound → HCID 9974054, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86747869 | HCID 86747869 | — |
| Solvent | Ethylacetate methanol | HCID 21584119 | — |
| Product | HCID 9974054 | HCID 9974054 | — |
Reaction Steps
The title compound was prepared according to Example 1(v) by using ethyl (E)-3-[2-n-butyl-1-{(2-chlorophenyl)methyl}-1H-imidazol-5-yl]-3-methyl-2-propenoate in place of ethyl-(E)-3-[2-n-butyl-1-{(2-chlorgphenyl)methyl}-1H-imidazol-5-yl]-2-methyl-2-propenoate. The title compound was a white solid, and was converted to the hydrochloride salt to give 82 mg (41%); mp 198°-199.5° C. (from ethyl acetate/methanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05312828 |
| Source dataset | uspto-grants-1994_05 |
| ORD ID | ord-7903f81c2fa1499096d8c0904150d87b |
| Source note | uspto-grants-1994_05 |