Epichlorohydrin → HCID 20356588, compound

HRID 1033976Notes

Reaction equation

HRID 1033976 reaction equation
[CH2:1]([CH:3]1[O:5][CH2:4]1)[Cl:2].[O:6]1[CH2:10][CH2:9][CH2:8][CH2:7]1>>[CH2:1]([CH:3]1[O:5][CH2:4]1)[Cl:2].[CH2:9]1[CH2:10][O:6][CH2:7][CH2:8]1

Participants

3

Reactant 2

HCID 7835EpichlorohydrinHCID 8028Tetrahydrofuran

Product 1

HCID 20356588HCID 20356588, compoundYield 87%

Procedure

This procedure followed that outlined in Example 26 except that the monomer feed consisted of a 50:50 mixture of neat epichlorohydrin and THF (tetrahydrofuran). The solution was added over 40 hours at 0° C. to yield the copolymer in 87% yield. This was contaminated with 17% oligomer.

Workup

  1. additionThe solution was added over 40 hours at 0° C.
  2. customto yield the copolymer in 87% yield

Sources & evidence

ORD record
ord-a68ecc328bbf4ef6affc3e04f766714d
Source dataset
uspto-grants-1994_05
Patent number
US05313000

Reaction notes

Loading…