HRID1034050

反应详情

EQUATION

反应方程式

HRID 1034050 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

CONDITIONS

反应条件

温度
25 °C

PROCEDURE

实验过程

A mixture of bis(3-isobutylphenyl)methanol (2.87 g) and oxaly chloride (1 ml) in dichloromethane (10 ml) was stirred at 25° C. for 2 hours. After evaporation of the solvent, the oily residue was distilled to give bis(3-isobutylphenyl)chloromethane (2.45 g) as pale yellow oil.

WORKUP

后处理

  1. customAfter evaporation of the solvent
  2. distillationthe oily residue was distilled