Chloride → Bis(3-isobutylphenyl)chloromethane
Reaction equation
[CH2:1]([C:5]1[CH:6]=[C:7]([CH:11]([C:13]2[CH:18]=[CH:17][CH:16]=[C:15]([CH2:19][CH:20]([CH3:22])[CH3:21])[CH:14]=2)O)[CH:8]=[CH:9][CH:10]=1)[CH:2]([CH3:4])[CH3:3].[Cl-:23]>ClCCl>[CH2:1]([C:5]1[CH:6]=[C:7]([CH:11]([C:13]2[CH:18]=[CH:17][CH:16]=[C:15]([CH2:19][CH:20]([CH3:22])[CH3:21])[CH:14]=2)[Cl:23])[CH:8]=[CH:9][CH:10]=1)[CH:2]([CH3:4])[CH3:3]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Conditions
- Temperature
- 25 °C
Procedure
A mixture of bis(3-isobutylphenyl)methanol (2.87 g) and oxaly chloride (1 ml) in dichloromethane (10 ml) was stirred at 25° C. for 2 hours. After evaporation of the solvent, the oily residue was distilled to give bis(3-isobutylphenyl)chloromethane (2.45 g) as pale yellow oil.
Workup
- customAfter evaporation of the solvent
- distillationthe oily residue was distilled
Sources & evidence
- ORD record
- ord-a2cd6472c4074f0b85ef8e826bd01609
- Source dataset
- uspto-grants-1994_05
- Patent number
- US05312829
Reaction notes
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