Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 19024738 | HCID 19024738 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19024785 | HCID 19024785 | — |
Reaction Steps
To a solution of 4-[2,2-bis(4-isobutylphenyl)ethyl]benzoic acid (400 mg) in dichloromethane (10 ml) were added oxalyl chloride (0.1 ml) and a drop of N,N-dimethylformamide at 0° C. After stirred at 20° C. for 1 hour, the,mixture was evaporated to give 4-[2,2-bis(4-isobutylphenyl)ethyl]benzoyl chloride (450 mg) as pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05312829 |
|---|
| Source dataset | uspto-grants-1994_05 |
|---|
| ORD ID | ord-c76f800a6ebb4d7aaee44843fad9cec2 |
|---|
| Source note | uspto-grants-1994_05 |
|---|
