Butylamine → HCID 19023630, compound

Participants

Reaction Steps

2.45 g of 2-[(4-chlorobutyl)sulfonyl]benzaldehyde was treated with 1.1 ml of n-butylamine, 3.4 g of magnesium sulfate, and 2 drops of concentrated sulfuric acid in 20 ml of diethyl ether in the same manner as described for Example 1, Part C to give 2.76 g of product. 1H-NMR (CDCl3) δ 0.96(t,3H,J=7 Hz); 1.32-1.50(m,2H); 1.65-1.79(m,2H); 1.84-1.93(m,4H); 3.11-3.20(m,2H); 3.46-3.53(m,2H); 3.67-3.74(m,2H); 7.55-7.73(m,2H); 8.00-8.13(m,2H); 9.12(s,1H).

Provenance & Evidence