HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19023733, compound → 1,2-Benzenediamine, N1-[(4-chlorophenyl)methyl]-4-(trifluoromethyl)-, hydrochloride (1:1)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19023733 | HCID 19023733 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1,2-Benzenediamine, N1-[(4-chlorophenyl)methyl]-4-(trifluoromethyl)-, hydrochloride (1:1) | HCID 19023737 | — |
Reaction Steps
A solution of 2-(4-chlorobenzylamino)-5-trifluoromethylnitrobenzene (70 g, 0.21 mmol) in ethanol (500 ml) was hydrogenated at a pressure of 4 bar. When the reaction was finished the product was filtered through a plug of celite into a flask containing 25 ml conc. HCl. After evaporation the product was suspended in petrol ether and filtered off. Yield 57 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05314903 |
| Source dataset | uspto-grants-1994_05 |
| ORD ID | ord-8dd7fe7d9ea3452e82d9b0e42f55e7ce |
| Source note | uspto-grants-1994_05 |