Cyclohexylamine → HCID 67821899, compound
Reaction equation
[CH:1]1([NH2:7])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.C[Al](C)C.[N:12]1([CH2:21][C:22]2[CH:23]=[C:24]([CH:30]=[CH:31][CH:32]=2)[C:25](OCC)=[O:26])[C:16]2[CH:17]=[CH:18][CH:19]=[CH:20][C:15]=2[N:14]=[CH:13]1>>[CH:1]1([NH:7][C:25](=[O:26])[C:24]2[CH:30]=[CH:31][CH:32]=[C:22]([CH2:21][N:12]3[C:16]4[CH:17]=[CH:18][CH:19]=[CH:20][C:15]=4[N:14]=[CH:13]3)[CH:23]=2)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1Participants
4
Procedure
N-Cyclohexyl 3-(1H-benzimidazylmethyl)benzamide was prepared by the method of example 9 starting with cyclohexylamine and reacting with trimethylaluminium and ethyl 3-(1H-benzimidazylmethyl)benzoate.
Sources & evidence
- ORD record
- ord-7809b714dd5c4387ae025749bd9ef0c6
- Source dataset
- uspto-grants-1994_05
- Patent number
- US05314880
Reaction notes
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