N-Methylcyclohexylamine → HCID 85612632, compound

HRID 1034280Notes

Reaction equation

HRID 1034280 reaction equation
[CH3:1][NH:2][CH:3]1[CH2:8][CH2:7][CH2:6][CH2:5][CH2:4]1.C[Al](C)C.[N:13]1([CH2:22][C:23]2[CH:24]=[C:25]([CH:31]=[CH:32][CH:33]=2)[C:26]([O:28]CC)=O)[C:17]2[CH:18]=[CH:19][CH:20]=[CH:21][C:16]=2[N:15]=[CH:14]1>>[CH:3]1([N:2]([CH3:1])[C:26](=[O:28])[C:25]2[CH:31]=[CH:32][CH:33]=[C:23]([CH2:22][N:13]3[C:17]4[CH:18]=[CH:19][CH:20]=[CH:21][C:16]=4[N:15]=[CH:14]3)[CH:24]=2)[CH2:8][CH2:7][CH2:6][CH2:5][CH2:4]1

Participants

4

Reactant 3

HCID 7514N-MethylcyclohexylamineHCID 16682925TrimethylaluminumHCID 67821870HCID 67821870, compound

Product 1

HCID 85612632HCID 85612632, compound

Procedure

N-Cyclohexyl-N-methyl 3-(1H-benzimidazylmethyl)benzamide was prepared by the method of Example 9 starting with N-methylcyclohexylamine and reacting with trimethylaluminium and ethyl 3-(1H-benzimidazylmethyl)benzoate.

Sources & evidence

ORD record
ord-9319eea44cc64be0bcd7b97443a3edff
Source dataset
uspto-grants-1994_05
Patent number
US05314880

Reaction notes

Loading…