N-Ethyl cyclohexylamine → HCID 85612634, compound

HRID 1034282Notes

Reaction equation

HRID 1034282 reaction equation
[CH2:1]([NH:3][CH:4]1[CH2:9][CH2:8][CH2:7][CH2:6][CH2:5]1)[CH3:2].C[Al](C)C.[N:14]1([CH2:23][C:24]2[CH:34]=[CH:33][C:27]([C:28]([O:30]CC)=O)=[CH:26][CH:25]=2)[C:18]2[CH:19]=[CH:20][CH:21]=[CH:22][C:17]=2[N:16]=[CH:15]1>>[CH:4]1([N:3]([CH2:1][CH3:2])[C:28](=[O:30])[C:27]2[CH:26]=[CH:25][C:24]([CH2:23][N:14]3[C:18]4[CH:19]=[CH:20][CH:21]=[CH:22][C:17]=4[N:16]=[CH:15]3)=[CH:34][CH:33]=2)[CH2:9][CH2:8][CH2:7][CH2:6][CH2:5]1

Participants

4

Reactant 3

HCID 21609N-Ethyl cyclohexylamineHCID 16682925TrimethylaluminumHCID 57061118HCID 57061118, compound

Product 1

HCID 85612634HCID 85612634, compound

Procedure

N-Cyclohexyl-N-ethyl 4-(1H-benzimidazylmethyl)benzamide was prepared by the method of Example 9 starting with N-ethylcyclohexylamine and reacting with trimethylaluminium and ethyl 4-(1H-benzimidazylmethyl)benzoate.

Sources & evidence

ORD record
ord-7b6e96f13c034fbd87d1beac2e4792bc
Source dataset
uspto-grants-1994_05
Patent number
US05314880

Reaction notes

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