HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl p-toluate → HCID 19023272, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl p-toluate | HCID 66743 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | N-Cyclohexyl-N,4-dimethylbenzenesulfonamide | HCID 614169 | — |
| Product | HCID 19023272 | HCID 19023272 | 90.1% |
Reaction Steps
Utilising the procedure described in Example 1(a) employing N-cyclohexyl-N-methyl 4-methylbenzenesulphonamide (20.0 g, 0.075 mol) in lieu of ethyl 4-methylbenzoate and two equivalents of NBS (27.0 g, 0.15 mol) yielded a crude product of N-cyclohexyl-N-methyl 4-bromomethylbenzenesulphonamide (23.4 g, 90%) as an orange oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05314880 |
| Source dataset | uspto-grants-1994_05 |
| ORD ID | ord-bdb763b948854923a02d346864ef977a |
| Source note | uspto-grants-1994_05 |