HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 3714618, compound → HCID 3714620, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 3714618 | HCID 3714618 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Platinum | HCID 23939 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 3714620 | HCID 3714620 | 98.9% |
Reaction Steps
A mixture of 13.16 g N-butyl-N-(3'-phenylpropyl)-4-hydroxy-3-nitrobenzenesulfonamide, 2 g 1 wt % platinum on alumina, and 200 ml ethanol was stirred for 22 hours at room temperature in a bomb charged with 800 psi of hydrogen. The solution was filtered and concentrated to give 12.02 g N-butyl-N-(3'-phenylpropyl)-3-amino-4-hydroxybenzensulfonamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05314998 |
| Source dataset | uspto-grants-1994_05 |
| ORD ID | ord-fd0a4dd1c9784b52b4acb02a8982fc26 |
| Source note | uspto-grants-1994_05 |