Methyl 10-methylacridan-9-carboxylate → HCID 68467549, compound

HRID 1034583Notes

Reaction equation

HRID 1034583 reaction equation
[CH3:1][N:2]1[C:15]2[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=2)[CH:9]([C:16]([O:18]C)=[O:17])[C:8]2[CH:7]=[CH:6][CH:5]=[CH:4][C:3]1=2>ClCCl.O1CCCC1>[CH3:1][N:2]1[C:15]2[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=2)[CH:9]([C:16]([OH:18])=[O:17])[C:8]2[CH:7]=[CH:6][CH:5]=[CH:4][C:3]1=2.[CH:13]1[CH:12]=[CH:11][C:10]([C:9]2[CH:16]=[CH:5][CH:6]=[CH:7][CH:8]=2)=[CH:15][CH:14]=1

Participants

4

Reactant 1

HCID 12813956Methyl 10-methylacridan-9-carboxylate

Product 1

HCID 68467549HCID 68467549, compound

Reagents, catalysts & solvents 2

HCID 6344DichloromethaneSolvent2×HCID 8028TetrahydrofuranSolvent

Procedure

A solution of 0.24 parts of 10-methylacridan-9-carboxylic acid chloride(78) in 10 mL dichloromethane and 0.145 parts of 4-phenylphenol (76) in 5 mL of dichloromethane and 1 mL of tetrahydrofuran is treated as described in example I, to give 0.21 parts of 4,4′-biphenyl 10-methylacridan-9-carboxylate. This compound has the following structure.

Sources & evidence

ORD record
ord-c1e3fe6f13a64e7a833e912c44c4ce33
Source dataset
uspto-grants-2013_10
Patent number
US08546150B2

Reaction notes

Loading…