Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 58093678 | HCID 58093678 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 58094187 | HCID 58094187 | — |
Reaction Steps
A mixture of 6,8-dichloro-2-methyl-2,7-naphthyridin-1(2H)-one (46 mg, 0.2 mmol) and CH3NH2 solution in THF (2.0 M, 2.5 mL) was heated at 95° C. for 5 hours and evaporated to afford the crude title compound. ESI-MS m/z 224.0 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08546370B2 |
|---|
| Source dataset | uspto-grants-2013_10 |
|---|
| ORD ID | ord-0d0d814bf81a4c25aee2e3f2a596c3df |
|---|
| Source note | uspto-grants-2013_10 |
|---|
