3-Hydroxypyridine → HCID 43087651, compound

HRID 1035049Notes

Reaction equation

[N:1]1[CH:6]=[CH:5][CH:4]=[C:3]([OH:7])[CH:2]=1.Cl[C:9]1[N:16]=[CH:15][CH:14]=[CH:13][C:10]=1[C:11]#[N:12]>>[N:1]1[CH:6]=[CH:5][CH:4]=[C:3]([O:7][C:9]2[N:16]=[CH:15][CH:14]=[CH:13][C:10]=2[C:11]#[N:12])[CH:2]=1

Participants

Reactant 2

HCID 79713-Hydroxypyridine

HCID 810792-Chloronicotinonitrile

Product 1

HCID 43087651HCID 43087651, compound

Procedure

Pyridin-3-ol was treated with 2-chloronicotinonitrile and processed according to the method of Example 128B to provide the product. MS (ESI+) m/z 198 (M+H)+.

Workup

customto provide the product

Sources & evidence

ORD record: ord-07d2d0f7f5644a199c1532846b9ac0b2
Source dataset: uspto-grants-2013_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08546374B2

Reaction notes

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