HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Bis(trifluoromethyl)aniline → 1-(2,3-Bis(trifluoromethyl)phenyl)-3-(2-fluoropyridin-3-ylmethyl)thiourea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Bis(trifluoromethyl)aniline | HCID 19980662 | — |
| Reactant | (2-Fluoropyridin-3-yl)methanamine | HCID 45079719 | — |
| Reactant | 2,3-Dichloro-1-fluorophenylisothiocyanate | HCID 86603533 | — |
| Product | 1-(2,3-Bis(trifluoromethyl)phenyl)-3-(2-fluoropyridin-3-ylmethyl)thiourea | HCID 86603532 | 90% |
Reaction Steps
Prepared in 90% yield from the product of Example 197A and the product of Example 193C according to the procedure described for the product of Example 192D and Example 192G.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546374B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-838514b9f9e14467ac8ce1415ec270e8 |
| Source note | uspto-grants-2013_10 |