2-Fluoropyridine-3-boronic acid → HCID 68584668, compound

Participants

Reaction Steps

The title compound was prepared from 2-fluoropyridine-3-boronic acid and the product of Example 285B using General Procedure 6. MS (ESI+) m/z 434.2 (M+H)+; Rt=1.87 min. 1H-NMR (400 MHz, DMSO-d6) δ 5.56 (s, 2H), 7.46 (m, 2H), 7.55 (m, 2H), 7.73 (dd, J=1.5 Hz, J=7.9 Hz, 1H), 7.98 (ddd, J=2.0 Hz, J=7.4 Hz, J=9.6 Hz, 1H), 8.31 (d, J=4.8 Hz, 1H), 8.68 (dd, J=1.61 Hz, J=4.7 Hz, 1H), 8.99 (s, 1H).

Provenance & Evidence