HRID1035248

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID17022

Benzaldehyde, 3-chloro-4-hydroxy- (8CI)(9CI)

C7H5ClO2

结构：CS(=O)(=O)OC1CN(C(=O)c2nnc(-c3ccccc3)o2)C1

HCID58043099

未命名化合物

PRODUCTS

生成物

结构：O=Cc1ccc(OC2CN(C(=O)c3nnc(-c4ccccc4)o3)C2)c(Cl)c1

HCID58043128

未命名化合物

收率 10%

PROCEDURE

实验过程

Using a similar protocol as described in Example 71A employing 53B and 3-chloro-4-hydroxybenzaldehyde as starting materials afforded 51 mg (10%) of 78A as a solid. 1H NMR (500 MHz, CDCl3): δ 4.44 (m, 1H), 4.75 (m, 1H), 4.87 (m, 1H), 5.22 (m, 2H), 6.75 (s, 1H), 7.53 (t, 2H), 7.61 (t, 1H), 7.80 (d, 1H), 7.98 (s, 1H), 8.18 (d, 2H), 9.90 (s, 1H).