HRID1035250

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID17022

Benzaldehyde, 3-chloro-4-hydroxy- (8CI)(9CI)

C7H5ClO2

结构：COc1ccc(-c2nnc(C(=O)N3CC(OS(C)(=O)=O)C3)o2)cc1

HCID58043131

未命名化合物

PRODUCTS

生成物

结构：COc1ccc(-c2nnc(C(=O)N3CC(Oc4ccc(C=O)cc4Cl)C3)o2)cc1

HCID58043141

未命名化合物

收率 15%

PROCEDURE

实验过程

Using a similar protocol as described in Example 71A employing 73B and 3-chloro-4-hydroxybenzaldehyde as starting materials afforded 80 mg (15%) of 79A as a solid. 1H NMR (500 MHz, CDCl3): δ 3.89 (s, 3H), 4.43 (m, 1H), 4.74 (m, 1H), 4.85 (m, 1H), 5.21 (m, 2H), 6.75 (s, 1H), 7.02 (d, 2H), 7.79 (d, 1H), 7.97 (s, 1H), 8.11 (d, 2H), 9.89 (s, 1H).