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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1035603Generated: November 1, 2026

HCID 24829226, compound → 3-(6-Methoxynaphthalen-2-yl)aniline

https://huagongshe.com/reaction/1035603

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 24829226HCID 24829226—
SolventTetrahydrofuranHCID 8028—
SolventPalladiumHCID 23938—
Product3-(6-Methoxynaphthalen-2-yl)anilineHCID 2272407420%

Reaction Steps

To a solution of 2-methoxy-6-(3-nitrophenyl)naphthalene (200 mg, 0.71 mmol, 1 eq) in 100 ml of dry THF, Pd/C is added, and the mixture is stirred over night at RT under a hydrogen atmosphere. After filtration over Celite and purification by means of preparative thin-layer chromatograph, the product is obtained in a yield of 20% (36 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08546392B2
Source datasetuspto-grants-2013_10
ORD IDord-81d3a3f1c3484e06afbb198bbe71142f
Source noteuspto-grants-2013_10