HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 24829226, compound → 3-(6-Methoxynaphthalen-2-yl)aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 24829226 | HCID 24829226 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Solvent | Palladium | HCID 23938 | — |
| Product | 3-(6-Methoxynaphthalen-2-yl)aniline | HCID 22724074 | 20% |
Reaction Steps
To a solution of 2-methoxy-6-(3-nitrophenyl)naphthalene (200 mg, 0.71 mmol, 1 eq) in 100 ml of dry THF, Pd/C is added, and the mixture is stirred over night at RT under a hydrogen atmosphere. After filtration over Celite and purification by means of preparative thin-layer chromatograph, the product is obtained in a yield of 20% (36 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546392B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-81d3a3f1c3484e06afbb198bbe71142f |
| Source note | uspto-grants-2013_10 |