HRID1035603

反应详情

EQUATION

反应方程式

HRID 1035603 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To a solution of 2-methoxy-6-(3-nitrophenyl)naphthalene (200 mg, 0.71 mmol, 1 eq) in 100 ml of dry THF, Pd/C is added, and the mixture is stirred over night at RT under a hydrogen atmosphere. After filtration over Celite and purification by means of preparative thin-layer chromatograph, the product is obtained in a yield of 20% (36 mg).

WORKUP

后处理

  1. filtrationAfter filtration
  2. customover Celite and purification by means of preparative thin-layer chromatograph
  3. customthe product is obtained in a yield of 20% (36 mg)