HRID1035605

反应详情

EQUATION

反应方程式

HRID 1035605 的结构方程式

PROCEDURE

实验过程

The compound is prepared by the reaction of 2-bromonaphthalene (303 mg, 1.46 mmol, 1 eq) with 3-hydroxyphenylboric acid (242 mg, 1.76 mmol, 1.2 eq) according to method A within 18 h. Purification by column chromatography with dichloromethane as the eluent yields the desired product in a yield of 47%, 152 mg.

WORKUP

后处理

  1. customPurification by column chromatography with dichloromethane as the eluent