HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromonaphthalene → 3-(2-Naphthyl)phenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromonaphthalene | HCID 11372 | — |
| Reactant | 3-Hydroxyphenylboric acid | HCID 21708183 | — |
| Product | 3-(2-Naphthyl)phenol | HCID 12316406 | 47% |
Reaction Steps
The compound is prepared by the reaction of 2-bromonaphthalene (303 mg, 1.46 mmol, 1 eq) with 3-hydroxyphenylboric acid (242 mg, 1.76 mmol, 1.2 eq) according to method A within 18 h. Purification by column chromatography with dichloromethane as the eluent yields the desired product in a yield of 47%, 152 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546392B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-9e869aec416448c1957e28defc419775 |
| Source note | uspto-grants-2013_10 |