HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,6-Dibromo-2-methoxynaphthalene → HCID 59443446, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,6-Dibromo-2-methoxynaphthalene | HCID 3503057 | — |
| Reactant | 3-Methoxyphenylboric acid | HCID 22173823 | — |
| Product | HCID 59443446 | HCID 59443446 | 81% |
Reaction Steps
The compound is prepared by the reaction of 1,6-dibromo-2-methoxy-naphthalene (5.75 g, 18.20 mmol, 1 eq) with 3-methoxyphenylboric acid (2.77 g, 18.20 mmol, 1 eq) according to method A. Purification by column chromatography with hexane as the eluent yielded the desired compound in a yield of 81%, 5.1 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546392B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-cec8634c05b8452995dbcc8c25b65f70 |
| Source note | uspto-grants-2013_10 |