HRID1035613

反应详情

EQUATION

反应方程式

HRID 1035613 的结构方程式

PROCEDURE

实验过程

The compound is prepared by the reaction of 1-bromo-6-(3-hydroxyphenyl)-naphthalene-2-ol (100 mg, 0.32 mmol, 1 eq) with 6-methoxypyridin-3-ylboric acid (48.6 mg, 0.32 mmol, 1 eq) according to method A in 3 h. Purification by column chromatography with hexane/ethyl acetate 8/2 yields the desired compound in a yield of 84%, 92 mg.

WORKUP

后处理

  1. customPurification by column chromatography with hexane/ethyl acetate 8/2