HRID1035613
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
The compound is prepared by the reaction of 1-bromo-6-(3-hydroxyphenyl)-naphthalene-2-ol (100 mg, 0.32 mmol, 1 eq) with 6-methoxypyridin-3-ylboric acid (48.6 mg, 0.32 mmol, 1 eq) according to method A in 3 h. Purification by column chromatography with hexane/ethyl acetate 8/2 yields the desired compound in a yield of 84%, 92 mg.
WORKUP
后处理
- customPurification by column chromatography with hexane/ethyl acetate 8/2