HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 24950391, compound → HCID 25069763, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 24950391 | HCID 24950391 | — |
| Reactant | HCID 67315140 | HCID 67315140 | — |
| Product | HCID 25069763 | HCID 25069763 | 84% |
Reaction Steps
The compound is prepared by the reaction of 1-bromo-6-(3-hydroxyphenyl)-naphthalene-2-ol (100 mg, 0.32 mmol, 1 eq) with 6-methoxypyridin-3-ylboric acid (48.6 mg, 0.32 mmol, 1 eq) according to method A in 3 h. Purification by column chromatography with hexane/ethyl acetate 8/2 yields the desired compound in a yield of 84%, 92 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546392B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-1b7144d5048f4d14afd27fa5fd46bc68 |
| Source note | uspto-grants-2013_10 |