反应详情

The compound is prepared by the reaction of 1-bromo-6-(3-hydroxyphenyl)-naphthalene-2-ol (150 mg, 0.48 mmol, 1 eq) with 4-morpholinophenylboric acid (98.6 mg, 0.48 mmol, 1 eq) according to method A in 21 h. Purification by column chromatography with dichloromethane/methanol 99/1 yields the desired compound in a yield of 7%, 13 mg.

1. customPurification by column chromatography with dichloromethane/methanol 99/1