HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 24950391, compound → HCID 25074168, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 24950391 | HCID 24950391 | — |
| Reactant | HCID 54337551 | HCID 54337551 | — |
| Product | HCID 25074168 | HCID 25074168 | 7% |
Reaction Steps
The compound is prepared by the reaction of 1-bromo-6-(3-hydroxyphenyl)-naphthalene-2-ol (150 mg, 0.48 mmol, 1 eq) with 4-morpholinophenylboric acid (98.6 mg, 0.48 mmol, 1 eq) according to method A in 21 h. Purification by column chromatography with dichloromethane/methanol 99/1 yields the desired compound in a yield of 7%, 13 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546392B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-8e6e3b2c639c427c876b776f17bcefbb |
| Source note | uspto-grants-2013_10 |