HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 25035958, compound → HCID 59443480, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 25035958 | HCID 25035958 | — |
| Reactant | HCID 68482452 | HCID 68482452 | — |
| Product | HCID 59443480 | HCID 59443480 | 14% |
Reaction Steps
The compound is prepared by the reaction of 3-bromo-N-(thiazol-2-yl)benzenesulfonamide (88.8 mg, 0.28 mmol, 1 eq) with 2-methoxy-6-(3-methoxyphenyl)-naphthalene-1-ylboric acid (100 mg, 0.36 mmol, 1.3 eq) according to method C. Purification by column chromatography with dichloromethane/methanol 95/5 yields the desired compound in a yield of 14%, 19 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546392B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-acc50a00d3ce4166b6e3e19895760671 |
| Source note | uspto-grants-2013_10 |