HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 59443448, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 59443487 | HCID 59443487 | — |
| Product | HCID 59443448 | HCID 59443448 | 28% |
Reaction Steps
The compound was prepared by reaction of 3-methoxy-5-(6-methoxy-naphthalene-2-yl)benzoic acid (500 mg, 1.62 mmol, 1 eq) with 33% methylamine solution (1 eq) according to method D. Purification by column chromatography with hexane/ethyl acetate 1/1 as the eluent yielded the desired product in a yield of 28%, 148 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546392B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-cdef42942964487d945b6091196ae624 |
| Source note | uspto-grants-2013_10 |