反应详情

The compound was prepared by reaction of 3-methoxy-5-(6-methoxy-naphthalene-2-yl)benzoic acid (500 mg, 1.62 mmol, 1 eq) with 33% methylamine solution (1 eq) according to method D. Purification by column chromatography with hexane/ethyl acetate 1/1 as the eluent yielded the desired product in a yield of 28%, 148 mg.

1. customPurification by column chromatography with hexane/ethyl acetate 1/1 as the eluent