HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → HCID 59443482, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | 2-Methoxy-6-(3-methoxyphenyl)-1-naphthoic acid | HCID 59443481 | — |
| Product | HCID 59443482 | HCID 59443482 | 85% |
Reaction Steps
The compound was prepared by reaction of 2-methoxy-6-(3-methoxyphenyl)-1-naphthoic acid (300 mg, 0.97 mmol, 1 eq) with aniline (1 eq) according to method D. Purification by column chromatography with hexane/ethyl acetate 2/1 as the eluent yielded the desired compound in a yield of 85%, 316 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546392B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-22625dd9c772478c8865cba6c2e207ce |
| Source note | uspto-grants-2013_10 |