HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3,4-Thiadiazole, 2-amino-5-methyl- → 2-Methoxy-6-(3-methoxyphenyl)-N-(5-methyl-1,3,4-thiadiazol-2-yl)-1-naphthamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3,4-Thiadiazole, 2-amino-5-methyl- | HCID 66949 | — |
| Reactant | HCID 59443481 | HCID 59443481 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 2-Methoxy-6-(3-methoxyphenyl)-N-(5-methyl-1,3,4-thiadiazol-2-yl)-1-naphthamide | HCID 59443476 | — |
Reaction Steps
The compound was prepared by reaction of 2-methoxy-6-(3-methoxyphenyl)-1-naphthoic acid (450 mg, 1.46 mmol, 1 eq) with 2-amino-5-methyl-1,3,4-thiadiazole (0.6 eq) according to method E. Characterization of the compound was not effected. The raw product was directly employed for ether cleavage.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546392B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-13c911293eaf4529b06fe5f7c0e34114 |
| Source note | uspto-grants-2013_10 |