HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron tribromide → HCID 24827434, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | HCID 13408303 | HCID 13408303 | — |
| Product | HCID 24827434 | HCID 24827434 | 76% |
Reaction Steps
The compound is prepared by reaction of 5-methoxy-2-(3-methoxyphenyl)-1H-indole (89 mg, 0.35 mmol, 1 eq) with boron tribromide (2.1 ml, 2.1 mmol, 6 eq) according to method G. Purification by preparative thin-layer chromatography with hexane/ethyl acetate 4/6 yields the desired product in a yield of 76%, 60 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546392B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-c0d56c57fa9d493daca45d1c1392f9e5 |
| Source note | uspto-grants-2013_10 |