Aluminum(III) Chloride → HCID 24827431, compound

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Reaction Steps

The compound is prepared by reaction of 3-methoxy-5-(6-methoxynaphthalene-2-yl)pyridine (200 mg, 0.75 mmol, 1 eq) with aluminum trichloride (803 mg, 6.04 mmol, 8 eq) according to method F. Purification by column chromatography with dichloromethane/methanol 95/5 as the eluent yields the desired product in a yield of 7%, 13 mg.

Provenance & Evidence