HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron tribromide → HCID 10308021, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | HCID 24829224 | HCID 24829224 | — |
| Product | HCID 10308021 | HCID 10308021 | 30% |
Reaction Steps
The compound is prepared by reaction of 6-(4-methoxyphenyl)-1-naphthol (57 mg, 0.23 mol, 1 eq) with boron tribromide (2.3 ml, 2.28 mmol, 10 eq) according to method G. Purification by column chromatography with dichloromethane/2% methanol as the eluent yields the desired product in a yield of 30%, 16 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546392B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-c10f85f3a9ee40a8bcad2618573000b3 |
| Source note | uspto-grants-2013_10 |