HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron tribromide → HCID 24950040, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | HCID 59443448 | HCID 59443448 | — |
| Product | HCID 24950040 | HCID 24950040 | — |
Reaction Steps
The compound is prepared by reaction of 3-methoxy-5-(6-methoxynaphthalene-2-yl)-N-methylbenzamide (110 mg, 0.34 mmol, 1 eq) with boron tribromide solution (5 eq) according to method G. Purification by column chromatography was not necessary. The desired product was already obtained after the processing in quantitative yield (99.6 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546392B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-a1841642b61f46fca08cdaff73e63132 |
| Source note | uspto-grants-2013_10 |