HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminum(III) Chloride → HCID 24950220, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | HCID 59443468 | HCID 59443468 | — |
| Product | HCID 24950220 | HCID 24950220 | 23% |
Reaction Steps
The compound is prepared by reaction of 3-[3-methoxy-5-(6-methoxy-naphthalene-2-yl)phenyl]-N-phenylpropionamide (55 mg, 0.13 mmol, 1 eq) with aluminum trichloride (291.3 mg, 2.19 mmol, 12 eq) according to method F. Purification by preparative thin-layer chromatography with hexane/ethyl acetate 1/1 yielded the desired product in a yield of 23%, 17 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546392B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-6f9471f2f96d4083b51016acb5b238ac |
| Source note | uspto-grants-2013_10 |