HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron tribromide → HCID 25074167, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | HCID 50942707 | HCID 50942707 | — |
| Product | HCID 25074167 | HCID 25074167 | — |
Reaction Steps
The compound is prepared by the reaction of 3-(2-methoxy-6-(3-methoxyphenyl)naphthalene-1-yl)benzeneamine (1 g, 2.82 mmol, 1 eq) with boron tribromide solution (14.1 ml, 14.1 mmol, 5 eq) according to method G. Purification by column chromatography was not necessary, and the desired product was obtained in quantitative yield (922 mg) after processing.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546392B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-cb78ca08082f411b958f7569a3ea1d0b |
| Source note | uspto-grants-2013_10 |