Boron tribromide → HCID 59443461, compound

HRID 1035681Notes

Reaction equation

HRID 1035681 reaction equation
C[O:2][C:3]1[CH:12]=[CH:11][C:10]2[C:5](=[CH:6][CH:7]=[C:8]([C:13]3[CH:18]=[CH:17][CH:16]=[C:15]([O:19]C)[CH:14]=3)[CH:9]=2)[C:4]=1[S:21][C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1.B(Br)(Br)Br>C1CCCCC1>[OH:19][C:15]1[CH:14]=[C:13]([C:8]2[CH:9]=[C:10]3[C:5](=[CH:6][CH:7]=2)[C:4]([S:21][C:22]2[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=2)=[C:3]([OH:2])[CH:12]=[CH:11]3)[CH:18]=[CH:17][CH:16]=1

Participants

4

Reactant 2

HCID 25134Boron tribromideHCID 59443474HCID 59443474, compound

Product 1

HCID 59443461HCID 59443461, compound

Reagents, catalysts & solvents 1

HCID 8078CyclohexaneSolvent

Procedure

The compound was prepared by reacting 2-methoxy-6-(3-methoxyphenyl)-1-(phenylsulfanyl)naphthalene (376 mg, 1.01 mmol, 1 eq.) with boron tribromide (8 ml of a 1 M solution in cyclohexane, 8 mmol, 8 eq) according to method G. Yield: 325 mg (94%)

Workup

  1. customThe compound was prepared

Sources & evidence

ORD record
ord-87aba4ee2f834bd494d0efc7970614b5
Source dataset
uspto-grants-2013_10
Patent number
US08546392B2

Reaction notes

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