HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron tribromide → HCID 59443461, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | HCID 59443474 | HCID 59443474 | — |
| Solvent | Cyclohexane | HCID 8078 | — |
| Product | HCID 59443461 | HCID 59443461 | — |
Reaction Steps
The compound was prepared by reacting 2-methoxy-6-(3-methoxyphenyl)-1-(phenylsulfanyl)naphthalene (376 mg, 1.01 mmol, 1 eq.) with boron tribromide (8 ml of a 1 M solution in cyclohexane, 8 mmol, 8 eq) according to method G. Yield: 325 mg (94%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546392B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-87aba4ee2f834bd494d0efc7970614b5 |
| Source note | uspto-grants-2013_10 |