HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-2-methoxybenzaldehyde → HCID 67067707, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-2-methoxybenzaldehyde | HCID 11053041 | — |
| Reactant | 1-(5-Fluoro-2-methoxy-phenyl)-3-phenyl-prop-2-yn-1-ol | HCID 67067672 | — |
| Product | HCID 67067707 | HCID 67067707 | 96% |
Reaction Steps
Following the procedure used to prepare 1-(5-fluoro-2-methoxy-phenyl)-3-phenyl-prop-2-yn-1-ol, 2-methoxy-4-bromobenzaldehyde was reacted to give the title compound as a pale yellow oil (1.43 g, 96%). LCMS (Method B): RT=4.53 min, [M+H]+=299/301.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546376B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-d3e28966f685416cadb22b71d0614cd5 |
| Source note | uspto-grants-2013_10 |