HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11718442, compound → HCID 67067743, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11718442 | HCID 11718442 | — |
| Reactant | {1-[4-(6-Fluoro-4-oxo-2-phenyl-4H-chromen-3-yl)-phenyl]-cyclobutyl}-carbamic acid tert-butyl ester | HCID 67067635 | — |
| Product | HCID 67067743 | HCID 67067743 | 86% |
Reaction Steps
Following the procedure used to prepare {1-[4-(6-fluoro-4-oxo-2-phenyl-4H-chromen-3-yl)-phenyl]-cyclobutyl}-carbamic acid tert-butyl ester, 3-iodo-6,7-dimethoxy-2-phenyl-chromen-4-one was reacted to give the title compound as a white solid (68 mg, 86%). LCMS (Method B): RT=4.81 min, [M+H]+=528.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546376B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-05cd93da6dc2490798a9b3fef479033b |
| Source note | uspto-grants-2013_10 |