HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Dimethoxybenzaldehyde → HCID 67067745, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Dimethoxybenzaldehyde | HCID 66581 | — |
| Reactant | 1-(5-Fluoro-2-methoxy-phenyl)-3-phenyl-prop-2-yn-1-ol | HCID 67067672 | — |
| Product | HCID 67067745 | HCID 67067745 | 66% |
Reaction Steps
Following the procedure used to prepare 1-(5-fluoro-2-methoxy-phenyl)-3-phenyl-prop-2-yn-1-ol, 2,3-dimethoxybenzaldehyde was reacted to give the title compound as a colourless oil (352 mg, 66%). LCMS (Method B): RT=4.09 min, [M+Na]+=291.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546376B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-f55ee837c029486e84fd6d38624c310d |
| Source note | uspto-grants-2013_10 |