HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromo-2,4-dimethoxybenzaldehyde → HCID 67067675, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromo-2,4-dimethoxybenzaldehyde | HCID 668346 | — |
| Reactant | 1-(5-Fluoro-2-methoxy-phenyl)-3-phenyl-prop-2-yn-1-ol | HCID 67067672 | — |
| Product | HCID 67067675 | HCID 67067675 | 100% |
Reaction Steps
Following the procedure used to prepare 1-(5-fluoro-2-methoxy-phenyl)-3-phenyl-prop-2-yn-1-ol, 2,4-dimethoxy-5-bromobenzaldehyde was reacted to give the title compound as a yellow foam (1.43 g, 100%). LCMS (Method B): RT=4.99 min, [M+Na]+=369/371.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546376B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-b45ac040c0624aadbeb2f7d4bda1421a |
| Source note | uspto-grants-2013_10 |