HRID1037289

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID11523469

6-FLUORO-3-IODO-2-PHENYLCHROMEN-4-ONE

C15H8FIO2

结构：COc1c(C(=O)C#Cc2ccccc2)ccc2cnn(S(=O)(=O)N(C)C)c12

HCID67067758

未命名化合物

结构：CN(C)S(=O)(=O)n1ncc2ccc3c(=O)c(I)c(-c4ccccc4)oc3c21

HCID67067832

未命名化合物

PRODUCTS

生成物

结构：NC1(c2ccc(-c3c(-c4ccccc4)oc4c(ccc5cn[nH]c54)c3=O)cc2)CCC1

HCID51029949

未命名化合物

收率 82%

PROCEDURE

实验过程

7-Iodo-6-oxo-8-phenyl-6H-9-oxa-1,2-diaza-cyclopenta[a]naphthalene-1-sulfonic acid dimethylamide Following the procedure used to prepare 6-fluoro-3-iodo-2-phenyl-chromen-4-one, 7-methoxy-6-(3-phenyl-propynoyl)-indazole-1-sulfonic acid dimethylamide was reacted to give the title compound as a tan solid (173 mg, 82%). LCMS (Method B): RT=4.42 min, [M+H]+=496.

WORKUP

后处理

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