HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(5-Fluoro-2-methoxy-phenyl)-3-phenyl-prop-2-yn-1-ol → HCID 67067891, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(5-Fluoro-2-methoxy-phenyl)-3-phenyl-prop-2-yn-1-ol | HCID 67067672 | — |
| Reactant | HCID 86671053 | HCID 86671053 | — |
| Product | HCID 67067891 | HCID 67067891 | 91% |
Reaction Steps
Following the procedure used to prepare 1-(5-fluoro-2-methoxy-phenyl)-3-phenyl-prop-2-yn-1-ol, 2,3-dimethoxy-4-nitro-benzaldehyde was reacted to give the title compound as a colourless oil (1.42 g, 91%). LCMS (Method G): RT=3.66 min, [M−OH+H]+=297.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546376B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-8329634fc224446184cbe033fd610eec |
| Source note | uspto-grants-2013_10 |